(2,6-Mes2C6H3In)2(μ-Cl)2Cl2

Base Information

• Chemical Name: (2,6-Mes2C6H3In)2(μ-Cl)2Cl2
• CAS No.: 1196700-65-8
• Molecular Formula: C₄₈H₅₀Cl₄In₂
• Molecular Weight: 998.377

Synonyms:

Chemical Property of (2,6-Mes2C6H3In)2(μ-Cl)2Cl2

Chemical Property:

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Technology Process of (2,6-Mes2C6H3In)2(μ-Cl)2Cl2

There total 1 articles about (2,6-Mes2C6H3In)2(μ-Cl)2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

indium(III) chloride (10025-82-8) + (2,6-dimesitylphenyl)lithium → (2,6-Mes2C6H3In)2(μ-Cl)2Cl2 (1196700-65-8)

Guidance literature:

In diethyl ether; addn. of ethereal soln. lithium compd. to ethereal soln. of indium compd. at -78°C, warming to room temp., stirring overnight; evapn., extn. (warm hexane), filtration, concg., heating to dissolve ppt., crystn., elem. anal.;

DOI:10.1021/om9007967

Reference yield: 83.0%

(2,6-Mes2C6H3In)2(μ-Cl)2Cl2 (1196700-65-8) + sodium hydroxide (1310-73-2) → (2,6-Mes2C6H3In)2(μ-hydroxide)2Cl2

Guidance literature:

In sodium hydroxide; diethyl ether; aq. NaOH; addn. of aq. NaOH to ethereal soln. of indium compd., stirring at room temp. for 12 h; separating organic layer, drying over Na2SO4, evapn., recrystn. (CH2Cl2/hexane (1:3)), elem. anal.;

DOI:10.1021/om9007967

Reference yield: 80.0%

(2,6-Mes2C6H3In)2(μ-Cl)2Cl2 (1196700-65-8) + sodium hydroxide (1310-73-2) → (2,6-Mes2C6H3In)3(μ-hydroxide)4Cl2

Guidance literature:

In sodium hydroxide; toluene; aq. NaOH; addn. of aq. NaOH to toluene soln. of indium compd., stirring at room temp. overnight; separating organic layer, drying over Na2SO4, evapn., recrystn. (CHCl3/hexane (1:3)), elem. anal.;

DOI:10.1021/om9007967

upstream raw materials:

indium(III) chloride

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