trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II)

Base Information

Chemical Name:trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II)
CAS No.:110173-82-5
Molecular Formula:C₃₂H₂₆Cl₂N₄P₂Pd
Molecular Weight:705.859
Hs Code.:

Synonyms:

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Chemical Property of trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II)

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II)

There total 4 articles about trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 68469-71-6
2,2'-(phenylphosphanediyl)dipyridine

: palladium dichloride

: 110173-82-5,110222-28-1
PdCl₂(P(C₆H₅)(C₅H₄N)2)2

Guidance literature:: In acetonitrile; warming slurry of PdCl2 in anhydrous CH3CN to 50°C until dissolution was complete, addn. of soln. of PC6H5(C5H5N)2 in CH3CN, stirring for 20 h at 25°C, filtration by presence of pptn., concentrating soln. in vac.;; recrystn. from CH2Cl2/C6H12, pure product obtained;;

Reference yield: 95.0%

: 110173-82-5,110222-28-1
PdCl₂(P(C₆H₅)(C₅H₄N)2)2

: 110222-28-1,110173-82-5
trans-dichlorobis(di-2-pyridylphenylphosphine)palladium(II)

Guidance literature:: With PC₆H₅(C₅H₄N)2; In acetonitrile; refluxing soln. of PdCl2(PC6H5(C5H4N)2)2 and PC6H5(C5H5N)2 in CH3CN for 24 h, concg. in vac.;; chromatography on silica gel column with CH2Cl2;;

Reference yield: 70.0%

: sodium tetrachloropalladate(II)

: 68469-71-6
2,2'-(phenylphosphanediyl)dipyridine

: 110173-82-5,110222-28-1
PdCl₂(P(C₆H₅)(C₅H₄N)2)2

: C₂₁H₁₈Cl₂N₃PPd

Guidance literature:: In methanol; warming soln. of PC6H5(C5H5N)2 and NaPdCl4 in anhydrous methanol for 3-6 h, filtration, cooling to 25°C overnight, filtration;; recrystn. of first pptn. from CH3OH is shown to be pure PdCl2(PC6H5(C5H4N)2)(C6H5N); second pptn. is shown to be PdCl2(PC6H5(C5H4N)2)2, recrystn.; elem. anal.;;