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Cp2Y[OCPh2(C5H4)](THF)

Base Information Edit
  • Chemical Name:Cp2Y[OCPh2(C5H4)](THF)
  • CAS No.:1252609-33-8
  • Molecular Formula:C32H33O2Y
  • Molecular Weight:538.519
  • Hs Code.:
  • Mol file:1252609-33-8.mol
Cp<sub>2</sub>Y[OCPh<sub>2</sub>(C<sub>5</sub>H<sub>4</sub>)](THF)

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Chemical Property of Cp2Y[OCPh2(C5H4)](THF) Edit
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Technology Process of Cp2Y[OCPh2(C5H4)](THF)

There total 1 articles about Cp2Y[OCPh2(C5H4)](THF) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; toluene; (N2) Ph2CO was added to soln. Cp3Y in toluene, stirred at 85°C for 8 h, THF was added and stirred for 2 h; soln. was evapd. in vacuo, residue was washed with hexane, dissolved in THF, hexane diffusion; elem. anal.;
DOI:10.1021/om100755s
Guidance literature:
With n-BuLi; In tetrahydrofuran; hexane; (N2) n-BuLi in hexane was added dropwise to soln. Y complex in THF at -30°C, stirred for 30 min and slowly warmed to room temp. and stirred overnight; solvent was removed in vacuo, residue was extd. with toluene, solvent was evapd. in vacuo, residue was dissolved in THF, hexane diffusion; elem.anal.;
DOI:10.1021/om100755s
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