26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.1^5,9.1^10,13.1^15,18.1^19,23.1^24,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one

Base Information

• Chemical Name: 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.1^5,9.1^10,13.1^15,18.1^19,23.1^24,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one
• CAS No.: 138286-14-3
• Molecular Formula: C₄₄H₃₆N₈O₂
• Molecular Weight: 708.822
• Mol file: 138286-14-3.mol

Synonyms:

Chemical Property of 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.1^5,9.1^10,13.1^15,18.1^19,23.1^24,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.1^5,9.1^10,13.1^15,18.1^19,23.1^24,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one

There total 1 articles about 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.1^5,9.1^10,13.1^15,18.1^19,23.1^24,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.5%

1,3-di(aminomethyl)benzene (1477-55-0) + 1,3-bis<1-benzyl-5-methyl-4-((2-hydroxyimino)-1,3-dioxobutyl)-imidazol-2-yl>benzene (137389-52-7) → 3,11-Dibenzyl-2,12,16,26-tetramethyl-3,11,17,25,29,31,32,34-octaazaheptacyclo<24.2.1.15,9.110,13.115,18.119,23.124,27>octacosa-1,4(29),5(30),6,8,10(31),12,15,17,19,21,23(33),24,26-tetradecaene-14,28-dione (137389-54-9) + C88H72N16O4 (138286-16-5) + 26-acetyl-3,11-dibenzyl-2,12,16-trimethyl-3,11,17,25,28,30,31,33-octaazaheptacyclo<23.2.1.15,9.110,13.115,18.119,23.124,27>tritriaconta-1,4(28),5(29),6,8,10(30),12,15,17,19,21,23(32),24,26-tetradecaen-14-one (138286-14-3) + 15,25-diacetyl-3,11-dibenzyl-2,12-dimethyl-3,11,16,24,27,29,30,32-octaazaheptacyclo<22.2.1.15,9.110,13.114,17.118,22.123,26>dotriaconta-1,4(27),5(28),6,8,10(29),12,14,16,18,20,22(31),23,25-tetradecaene (138286-15-4)

Guidance literature:

With pyridine; at 105 ℃; for 67h;

DOI:10.1021/jo00030a038

upstream raw materials:

1,3-di(aminomethyl)benzene

1,3-bis<1-benzyl-5-methyl-4-((2-hydroxyimino)-1,3-dioxobutyl)-imidazol-2-yl>benzene