Technology Process of C27H25NO5S
There total 7 articles about C27H25NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H18O5S; 4-methoxy-aniline;
In
water; acetonitrile;
at 20 ℃;
for 8h;
Inert atmosphere;
In
water; acetonitrile;
at 120 ℃;
for 0.25h;
Inert atmosphere;
With
Amberlite IRC76 resin;
In
water; acetonitrile;
at 120 ℃;
for 0.25h;
Inert atmosphere;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 16 h / 65 °C / Inert atmosphere
2.1: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
3.1: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere
4.1: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
5.1: water; acetonitrile / 8 h / 20 °C / Inert atmosphere
5.2: 0.25 h / 120 °C / Inert atmosphere
5.3: Amberlite IRC76 resin / 0.25 h / 120 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; stabilized 2-iodoxybenzoic acid; Au(OAc)3; tetrabutyl ammonium fluoride; triethylamine;
In
dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;
1.1: Sonogashira coupling;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
2.1: water; acetonitrile / 8 h / 20 °C / Inert atmosphere
2.2: 0.25 h / 120 °C / Inert atmosphere
2.3: Amberlite IRC76 resin / 0.25 h / 120 °C / Inert atmosphere
With
polystyrene supported 4-dimethylaminopyridine;
In
dichloromethane; water; acetonitrile;
DOI:10.1021/co300002x