[ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate

Base Information

Chemical Name:[ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate
CAS No.:1254729-59-3
Molecular Formula:C₃₂H₁₂BF₂₄*C₃₉H₃₀ClO₃P₂Ru
Molecular Weight:1608.36
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate

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Technology Process of [ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate

There total 1 articles about [ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 201230-82-2
carbon monoxide

: 1254729-58-2
[ruthenium(II)(dicarbonyl)(fluoride)bis(triphenylphosphane)] hexaluorophosphate

: 105560-52-9
potassium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

: 1254729-59-3
[ruthenium(II)(tricarbonyl)(chloride)bis(triphenylphosphane)] tetra(3,5-bistrifluoromethylphenyl)borate

Guidance literature:: In dichloromethane; Schlenk technique, in dry box, under N2; CH2Cl2 added to Ru complex (0.237 mmol) and KB((CF3)2C6H3)4 (0.237 mmol) mixt., stirred at room temp. for 5 h, filtered, CO bubbled through stirred soln. at room temp. for 30 min; soln. added to Et2O, ppt. filtered off, recrystd. from CH2Cl2/hexane (1:100);
DOI:10.1002/ejic.201000410