C₂₅H₃₄ClN₃O₂S*ClH

Base Information

Chemical Name:C₂₅H₃₄ClN₃O₂S*ClH
CAS No.:1303527-38-9
Molecular Formula:C₂₅H₃₄ClN₃O₂S*ClH
Molecular Weight:512.544
Hs Code.:

C<sub>25</sub>H<sub>34</sub>ClN<sub>3</sub>O<sub>2</sub>S*ClH

Synonyms:

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Chemical Property of C₂₅H₃₄ClN₃O₂S*ClH

Chemical Property:

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Technology Process of C₂₅H₃₄ClN₃O₂S*ClH

There total 13 articles about C₂₅H₃₄ClN₃O₂S*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-56-8
i-propyl(2-(hydroxy)ethyl)amine

: 1303527-24-3
C₂₀H₂₂Cl₂N₂OS

: 1303527-38-9
C₂₅H₃₄ClN₃O₂S*ClH

Guidance literature:: With potassium carbonate; sodium iodide; In acetonitrile; at 160 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.bmcl.2011.02.023

Reference yield:

: 14774-37-9
(tetrahydro-2H-pyran-4-yl)methanol

: 1303527-38-9
C₂₅H₃₄ClN₃O₂S*ClH

Guidance literature:: Multi-step reaction with 9 steps

1: pyridine / 1.5 h / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide / 50 °C

3: oxalyl dichloride / 0 - 20 °C

4: ammonia; potassium carbonate / dichloromethane

5: tetraphosphorus decasulfide / tetrahydrofuran / 3 h / 55 °C

6: N,N-dimethyl-formamide / 0.5 h / 140 °C / Microwave irradiation

7: lithium borohydride / tetrahydrofuran / 2 h / 0 - 70 °C

8: methanesulfonylchloride; triethylamine / dichloromethane / 1 h

9: potassium carbonate; sodium iodide / acetonitrile / 0.08 h / 160 °C / Microwave irradiation

With pyridine; lithium borohydride; tetraphosphorus decasulfide; oxalyl dichloride; methanesulfonylchloride; ammonia; sodium hydride; potassium carbonate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.02.023

Reference yield:

: 53924-05-3
7-chloro-1H-indole

: 1303527-38-9
C₂₅H₃₄ClN₃O₂S*ClH

Guidance literature:: Multi-step reaction with 10 steps

1: N,N-dimethyl-formamide / 1 h / 0 - 20 °C

2: water; sodium hydroxide / 1 h / Reflux

3: sodium hydride / N,N-dimethyl-formamide / 50 °C

4: oxalyl dichloride / 0 - 20 °C

5: ammonia; potassium carbonate / dichloromethane

6: tetraphosphorus decasulfide / tetrahydrofuran / 3 h / 55 °C

7: N,N-dimethyl-formamide / 0.5 h / 140 °C / Microwave irradiation

8: lithium borohydride / tetrahydrofuran / 2 h / 0 - 70 °C

9: methanesulfonylchloride; triethylamine / dichloromethane / 1 h

10: potassium carbonate; sodium iodide / acetonitrile / 0.08 h / 160 °C / Microwave irradiation

With lithium borohydride; tetraphosphorus decasulfide; oxalyl dichloride; methanesulfonylchloride; ammonia; water; sodium hydride; potassium carbonate; triethylamine; sodium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.02.023