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Technology Process of 5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine

5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine

Base Information
  • Chemical Name:5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine
  • CAS No.:1218917-29-3
  • Molecular Formula:C52H74N7O7PS2Si
  • Molecular Weight:1032.39
  • Hs Code.:
5'-O-(4,4'-dimethoxytrityl)-N<sub>2</sub>-(tert-butyldithiopropyl)-O<sub>6</sub>-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine

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Chemical Property of 5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine
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Technology Process of 5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine

There total 1 articles about 5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

5'-O-(4,4'-dimethoxytrityl)-N<sub>2</sub>-(tert-butyldithiopropyl)-O<sub>6</sub>-(trimethylsilylethyl)-2'-deoxyinosine
1218917-28-2

5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-2'-deoxyinosine

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite
102691-36-1

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

5'-O-(4,4'-dimethoxytrityl)-N<sub>2</sub>-(tert-butyldithiopropyl)-O<sub>6</sub>-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine
1218917-29-3

5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl-2'-deoxyguanosine

Guidance literature:
With pyridinium trifluroacetate; In dichloromethane; for 4h; Inert atmosphere; Cooling with ice;
DOI:10.1080/15257770903368385
upstream raw materials:

5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-2'-deoxyinosine

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

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