2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester

Base Information

• Chemical Name: 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester
• CAS No.: 147699-02-3
• Molecular Formula: C₂₆H₂₇ClN₂O₇
• Molecular Weight: 514.963

Synonyms:

Chemical Property of 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester

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Technology Process of 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester

There total 3 articles about 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-Chloromethyl-1-(4-ethoxy-phenyl)-2-hydroxy-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester (147698-99-5) → 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester (147699-02-3)

Guidance literature:

In methanol; for 3h; Heating;

DOI:10.1007/BF02253029

Reference yield: 56.0%

4-Chloro-2-[1-(3-nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid methyl ester (107813-00-3) + (E)-3-(4-Ethoxy-phenylamino)-but-2-enoic acid ethyl ester → 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester (147699-02-3)

Guidance literature:

In methanol; for 2h; Heating;

DOI:10.1007/BF02253029

Reference yield: 55.0%

4-Chloro-2-[1-(3-nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid methyl ester (107813-00-3) + ethyl (Z)-3-(4-ethoxyphenylamino)but-2-enoate (920312-63-6) → 2-[1-Chloro-meth-(Z)-ylidene]-1-(4-ethoxy-phenyl)-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester (147699-02-3)

Guidance literature:

In methanol; for 2h; Heating;

DOI:10.1007/BF00474506

upstream raw materials:

4-Chloro-2-[1-(3-nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid methyl ester

ethyl (Z)-3-(4-ethoxyphenylamino)but-2-enoate

2-Chloromethyl-1-(4-ethoxy-phenyl)-2-hydroxy-6-methyl-4-(3-nitro-phenyl)-1,2,3,4-tetrahydro-pyridine-3,5-dicarboxylic acid 5-ethyl ester 3-methyl ester

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