1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene

Base Information

• Chemical Name: 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene
• CAS No.: 151340-07-7
• Molecular Formula: C₃₆H₃₀N₃O₇P₃
• Molecular Weight: 709.571
• Mol file: 151340-07-7.mol

Synonyms:

Chemical Property of 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene

There total 2 articles about 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C37H32N3O7P3 → 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene (151340-07-7)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.macromol.5b01892

Reference yield:

4-methoxy-phenol (150-76-5) → 1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene (151340-07-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 48 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.2: 24 h / Reflux; Inert atmosphere; Schlenk technique

3.1: boron tribromide / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With boron tribromide; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;

DOI:10.1021/acs.macromol.5b01892

Reference yield: 33.0%

1,1,3,3,5-pentaphenoxy-5-[(4-hydroxy)phenoxy]-cyclotriphosphazatriene (151340-07-7) + phthalocyanine silicon(IV) dichloride (19333-10-9) → C104H74N14O14P6Si

Guidance literature:

With sodium hydride; In toluene; for 10h; Inert atmosphere; Reflux;

DOI:10.1016/j.poly.2009.09.035

upstream raw materials:

4-methoxy-phenol