bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium

Base Information

• Chemical Name: bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium
• CAS No.: 1263381-83-4
• Molecular Formula: C₁₈H₂₂Cl₂GeN₄O₂
• Molecular Weight: 469.894
• Mol file: 1263381-83-4.mol

Synonyms:

Chemical Property of bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium

Chemical Property:

Purity/Quality:

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Technology Process of bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium

There total 1 articles about bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

germaniumtetrachloride (10038-98-9) + dimethylhydrazone of the trimethylsilyl ester of benzoic acid (112746-60-8) → bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium (1263381-83-4)

Guidance literature:

In chloroform; (Ar, Schlenk tecnique); stirring mixt. of germanium compd. and imidate deriv. in CHCl3 for 2 h at room temp.; evapn., washing with hexane, NMR;

DOI:10.1021/om101081u

upstream raw materials:

germaniumtetrachloride

dimethylhydrazone of the trimethylsilyl ester of benzoic acid