dimethylhydrazone of the trimethylsilyl ester of benzoic acid

Base Information

• Chemical Name: dimethylhydrazone of the trimethylsilyl ester of benzoic acid
• CAS No.: 112746-60-8
• Molecular Formula: C₁₂H₂₀N₂OSi
• Molecular Weight: 236.389

Synonyms:dimethylhydrazone of the trimethylsilyl ester of benzoic acid

Chemical Property of dimethylhydrazone of the trimethylsilyl ester of benzoic acid

Chemical Property:

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Technology Process of dimethylhydrazone of the trimethylsilyl ester of benzoic acid

There total 2 articles about dimethylhydrazone of the trimethylsilyl ester of benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chloro-trimethyl-silane (75-77-4) + 1-benzoyl-2,2-dimethylhydrazine (1128-86-5) → dimethylhydrazone of the trimethylsilyl ester of benzoic acid (112746-60-8)

Guidance literature:

With triethylamine; In benzene; 20 deg c, 2 h; reflux, 12 h;

DOI:10.1007/BF00957450

Reference yield:

O-trimethylsilyl-N-(triphenylphosphinimino)benzohydrazide + C24H27N4O2Si(1+)*Cl(1-) → bis[N-(triphenylphosphinimino)phenyl-N',O]phenylsiliconium chloride + dimethylhydrazone of the trimethylsilyl ester of benzoic acid (112746-60-8)

Guidance literature:

In chloroform-d1; at 20 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.poly.2015.08.011

Reference yield: 100.0%

dimethylhydrazone of the trimethylsilyl ester of benzoic acid (112746-60-8) → bis(N-(dimethylamino)benzimidato-N,O)chlorohydridosilicon(IV)

Guidance literature:

With trichlorosilane; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/ja00151a015

upstream raw materials:

chloro-trimethyl-silane

1-benzoyl-2,2-dimethylhydrazine

Downstream raw materials:

(Cl-Si)chloro<1-(1,1-dimethyl-2-benzoylhydrazonium)methyl>dimethylsilane

bis(N-(dimethylamino)benzimidato-N',O)dichlorogermanium

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