7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole

Base Information

Chemical Name:7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole
CAS No.:1265022-66-9
Molecular Formula:C₂₂H₂₁N₃O₃S
Molecular Weight:407.493
Hs Code.:

Synonyms:

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Chemical Property of 7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole

Chemical Property:

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Technology Process of 7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole

There total 3 articles about 7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 165669-35-2
7-bromo-1H-pyrrolo[2,3-c]pyridine

: 1265022-66-9
7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane / 0.5 h / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; ethanol / 24 h / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide; In ethanol; dichloromethane; toluene; 2.1: |Suzuki Coupling;
DOI:10.1021/jm4011115

Reference yield:

: 19755-53-4
2-bromo-3-nitropyridine

: 1265022-66-9
7-(4-(N,N-dimethylaminophenyl))-1-(4-methoxybenzenesulfonyl)-6-azaindole

Guidance literature:: Multi-step reaction with 3 steps

1.1: vinyl magnesium bromide / tetrahydrofuran / 1 h / -78 - -40 °C

2.1: potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane / 0.5 h / Inert atmosphere

2.2: 1 h / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / toluene; ethanol / 24 h / Reflux; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; vinyl magnesium bromide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; toluene; 3.1: |Suzuki Coupling;
DOI:10.1021/jm4011115