5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Base Information

Chemical Name:5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene
CAS No.:84735-07-9
Molecular Formula:C₃₇H₂₅N₃O₉
Molecular Weight:655.62
Hs Code.:

5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzo<de>naphthacene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

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Technology Process of 5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

There total 6 articles about 5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 108-24-7
acetic anhydride

: 84735-06-8
5-(7-hydroxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-2-phenyl-12-oxo-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

: 84735-07-9
5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: With pyridine; for 1h; boiling water bath;
DOI:10.1055/s-1982-30074

Reference yield:

: 5769-02-8
2-methyl-2-phenyl[1,3]dithiolane

: 84735-07-9
5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: Multi-step reaction with 4 steps

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 60 percent / pyridine / 1 h / boiling water bath

4: 80 percent / pyridine / 1 h / boiling water bath

With pyridine; ammonium acetate; In ethanol;
DOI:10.1055/s-1982-30074

Reference yield:

: 7338-51-4
7-hydroxy-5-methoxy-2-methyl-4-oxo-4H-chromene-6-carbaldehyde

: 84735-07-9
5-(7-Acetoxy-5-methoxy-2-methyl-4-oxo-4H-1-benzopyran-6-yl)-13-methoxy-10-methyl-12-oxo-2-phenyl-12H-7,9-dioxa-3,4,6-triazabenzonaphthacene

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / ammonium acetate / ethanol / 1 h

2: 65 percent / ammonium acetate / ethanol / 1 h / Heating

3: 60 percent / pyridine / 1 h / boiling water bath

4: 80 percent / pyridine / 1 h / boiling water bath

With pyridine; ammonium acetate; In ethanol;
DOI:10.1055/s-1982-30074