4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Base Information

Chemical Name:4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal
CAS No.:151963-91-6
Molecular Formula:C₃₅H₃₉NO₃S₂
Molecular Weight:585.832
Hs Code.:

Synonyms:

Suppliers and Price of 4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

There total 6 articles about 4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134700-11-1
3,4-di-O-benzyl-2-deoxy-D-erythro-pentose bisbenzyl dithioacetal

: 151963-91-6
4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / Ph₃P, DEAD / tetrahydrofuran / 5 h / Ambient temperature

2: 92 percent / K₂CO₃ / methanol / 2 h / Ambient temperature

3: 90 percent / pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 82 percent / NaN₃ / dimethylformamide / 3 h / 100 °C

5: LiAlH₄ / diethyl ether / 2 h / 0 °C

6: methanol / 12 h

With pyridine; lithium aluminium tetrahydride; sodium azide; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1993-25935

Reference yield:

: 134700-14-4
3,5-di-O-benzyl-2-deoxy-4-O-methanesulphonyl-L-threo-pentose dibenzyl dithioacetal

: 151963-91-6
4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / NaN₃ / dimethylformamide / 3 h / 100 °C

2: LiAlH₄ / diethyl ether / 2 h / 0 °C

3: methanol / 12 h

With lithium aluminium tetrahydride; sodium azide; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1055/s-1993-25935

Reference yield:

: 134700-12-2
4-O-benzoyl-3,5-di-O-benzyl-2-deoxy-L-threo-pentose dibenzyl dithioacetal

: 151963-91-6
4-acetamido-3,5-di-O-benzyl-2-deoxy-D-ribose dibenzyldithioacetal

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / K₂CO₃ / methanol / 2 h / Ambient temperature

2: 90 percent / pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 82 percent / NaN₃ / dimethylformamide / 3 h / 100 °C

4: LiAlH₄ / diethyl ether / 2 h / 0 °C

5: methanol / 12 h

With pyridine; lithium aluminium tetrahydride; sodium azide; potassium carbonate; In methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-1993-25935