C₆₃H₁₀₃N₁₁O₁₆Si₂

Base Information

Chemical Name:C₆₃H₁₀₃N₁₁O₁₆Si₂
CAS No.:473710-63-3
Molecular Formula:C₆₃H₁₀₃N₁₁O₁₆Si₂
Molecular Weight:1326.75
Hs Code.:

C<sub>63</sub>H<sub>103</sub>N<sub>11</sub>O<sub>16</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₆₃H₁₀₃N₁₁O₁₆Si₂

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Technology Process of C₆₃H₁₀₃N₁₁O₁₆Si₂

There total 10 articles about C₆₃H₁₀₃N₁₁O₁₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2018-66-8
Z-Leu-OH

: 473710-63-3
C₆₃H₁₀₃N₁₁O₁₆Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: HOBt; EDC; DIPA / tetrahydrofuran

2: HCl / tetrahydrofuran

3: NaBH(OAc)3; AcOH / tetrahydrofuran / 20 °C

4: H₂ / 10 percent Pd/C / methanol / 20 °C / atmospheric pressure

5: HOBt; EDC; Hunig base / tetrahydrofuran / 20 °C

With hydrogenchloride; hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; diisopropylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00671-1

Reference yield:

: 94226-56-9
tert-butyl 2-(dibenzylamino)ethanoate

: 473710-63-3
C₆₃H₁₀₃N₁₁O₁₆Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: LDA / tetrahydrofuran / 1 h / -78 °C

1.2: 31 percent / tetrahydrofuran / 17 h / -78 - -35 °C

2.1: H₂ / 10 percent Pd/C / methanol

3.1: NaBH(OAc)3; AcOH / tetrahydrofuran / 20 °C

4.1: H₂ / 10 percent Pd/C / methanol / 20 °C / atmospheric pressure

5.1: HOBt; EDC; Hunig base / tetrahydrofuran / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00671-1

Reference yield:

: 137233-53-5
2',3'-O-bis(tert-butyldimethylsilyl)-3-N-(p-methoxybenzyl)uridine-5'-aldehyde

: 473710-63-3
C₆₃H₁₀₃N₁₁O₁₆Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: LDA / tetrahydrofuran / 1 h / -78 °C

1.2: 31 percent / tetrahydrofuran / 17 h / -78 - -35 °C

2.1: H₂ / 10 percent Pd/C / methanol

3.1: NaBH(OAc)3; AcOH / tetrahydrofuran / 20 °C

4.1: H₂ / 10 percent Pd/C / methanol / 20 °C / atmospheric pressure

5.1: HOBt; EDC; Hunig base / tetrahydrofuran / 20 °C

With hydrogen; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1016/S0960-894X(03)00671-1