C₂₂H₂₉NOSi

Base Information

Chemical Name:C₂₂H₂₉NOSi
CAS No.:1427270-25-4
Molecular Formula:C₂₂H₂₉NOSi
Molecular Weight:351.564
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₉NOSi

Chemical Property:

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Technology Process of C₂₂H₂₉NOSi

There total 5 articles about C₂₂H₂₉NOSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88158-68-3
4-(tert-butyldiphenylsilyloxy)-1-butyne

: 1427270-25-4
C₂₂H₂₉NOSi

Guidance literature:: Multi-step reaction with 2 steps

1: ethylmagnesium bromide / tetrahydrofuran

2: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate

With phthalimide; di-isopropyl azodicarboxylate; ethylmagnesium bromide; triphenylphosphine; In tetrahydrofuran; 1: |Grignard Reaction / 2: |Gabriel Amine Synthesis / 2: |Gabriel Amine Synthesis;
DOI:10.1016/j.bmcl.2013.01.022

Reference yield:

: 122069-55-0
6-((tert-butyldiphenylsilyl)oxy)hex-3-yn-1-ol

: 1427270-25-4
C₂₂H₂₉NOSi

Guidance literature:: 6-((tert-butyldiphenylsilyl)oxy)hex-3-yn-1-ol; With phthalimide; di-isopropyl azodicarboxylate; triphenylphosphine;

With sodium tetrahydroborate; In water; isopropyl alcohol;
DOI:10.1016/j.bmcl.2013.01.022

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1427270-25-4
C₂₂H₂₉NOSi

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide

2: ethylmagnesium bromide / tetrahydrofuran

3: phthalimide; triphenylphosphine; di-isopropyl azodicarboxylate

With 1H-imidazole; phthalimide; di-isopropyl azodicarboxylate; ethylmagnesium bromide; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Grignard Reaction / 3: |Gabriel Amine Synthesis / 3: |Gabriel Amine Synthesis;
DOI:10.1016/j.bmcl.2013.01.022