p-benzoic acid

Base Information

• Chemical Name: p-benzoic acid
• CAS No.: 154825-45-3
• Molecular Formula: C₂₃H₂₉BrN₂O₃
• Molecular Weight: 461.399
• Mol file: 154825-45-3.mol

Synonyms:

Chemical Property of p-benzoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-benzoic acid

There total 1 articles about p-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1,10-dibromodecane (4101-68-2) + 4-(4-hydroxphenylazo)benzoic acid (105299-45-4,2497-38-3) → p-benzoic acid (154825-45-3)

Guidance literature:

DOI:10.1246/bcsj.57.3253

Reference yield: 68.0%

p-benzoic acid (154825-45-3) + (S)-octyl 2-aminopropanoate hydrochloride (171963-33-0) → (S)-2-{4-[4-(10-Bromo-decyloxy)-phenylazo]-benzoylamino}-propionic acid octyl ester

Guidance literature:

With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; Ambient temperature;

DOI:10.1039/p29960002707

Reference yield: 67.0%

p-benzoic acid (154825-45-3) + (S)-2-Amino-propionic acid tridecyl ester; hydrochloride → (S)-2-{4-[4-(10-Bromo-decyloxy)-phenylazo]-benzoylamino}-propionic acid tridecyl ester

Guidance literature:

With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; Ambient temperature;

DOI:10.1039/p29960002707

upstream raw materials:

1,10-dibromodecane

4-(4-hydroxphenylazo)benzoic acid

Downstream raw materials:

hexyl N-benzoyl>alaninate