{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 141287-75-4
• Molecular Formula: C₅₃H₇₃NO₆
• Molecular Weight: 820.166

Synonyms:

Chemical Property of {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

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Technology Process of {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

There total 2 articles about {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cholesterol (57-88-5) → {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (141287-75-4)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene / Ambient temperature

2: 78 percent / Et₃N / CH₂Cl₂

3: 44 percent / pyridine / 5 h

With pyridine; triethylamine; In dichloromethane; toluene;

DOI:10.1021/jm00022a025

Reference yield:

Cholesteryl chloroformate (7144-08-3) → {2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (141287-75-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / Et₃N / CH₂Cl₂

2: 44 percent / pyridine / 5 h

With pyridine; triethylamine; In dichloromethane;

DOI:10.1021/jm00022a025

Reference yield:

{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-(2-hydroxy-ethyl)-carbamic acid (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (141287-75-4) → C63H77F4NO9

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, N-methylimidazole / CH₂Cl₂

2: CH₂Cl₂ / 1 h

With 1-methyl-1H-imidazole; triethylamine; In dichloromethane;

DOI:10.1021/jm00022a025

upstream raw materials:

cholesterol

Cholesteryl chloroformate

Downstream raw materials:

C₅₇H₇₇NO₉

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