tetraphenyl-1,2-bis(acetoxy)distannane

Base Information

• Chemical Name: tetraphenyl-1,2-bis(acetoxy)distannane
• CAS No.: 30872-41-4
• Molecular Formula: C₂₈H₂₆O₄Sn₂
• Molecular Weight: 663.932
• Mol file: 30872-41-4.mol

Synonyms:

Chemical Property of tetraphenyl-1,2-bis(acetoxy)distannane

Chemical Property:

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Safty Information:

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Useful:

Technology Process of tetraphenyl-1,2-bis(acetoxy)distannane

There total 1 articles about tetraphenyl-1,2-bis(acetoxy)distannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

diphenyltin(IV) dichloride (1135-99-5) → tetraphenyl-1,2-bis(acetoxy)distannane (30872-41-4)

Guidance literature:

With LiAlH₄; acetic acid; In diethyl ether; byproducts: H2; Ph2SnCl2 (10.0 mmol) in ether added dropwise at 0°C to suspn. ofLiAlH4 (12.4 mmol) in ether, stirred for 1 h, hydrolyzed with H2O, org.phase sepd., dried with Na2SO4, treated with 96% CH3COOH (8.47 mmol); concd. at gentle heating, cooled in refrigerator; elem. anal.;

DOI:10.1016/0022-328X(87)80155-9

upstream raw materials:

diphenyltin(IV) dichloride