(5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid

Base Information

Chemical Name:(5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid
CAS No.:224448-58-2
Molecular Formula:C₃₁H₃₃NO₇
Molecular Weight:531.606
Hs Code.:

(5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid

Chemical Property:

Vapor Pressure:6.46E-21mmHg at 25°C

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Technology Process of (5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid

There total 4 articles about (5S,6R,7R)-5-(1,3-benzodioxol-5-yl)-2-butyl-7-{2-[(2S)-2-carboxypropyl]-4-methoxyphenyl}-6,7-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 247042-78-0
(5S,6R,7R)-5-Benzo[1,3]dioxol-5-yl-2-butyl-7-[2-((S)-3-hydroxy-2-methyl-propyl)-4-methoxy-phenyl]-6,7-dihydro-5H-[1]pyrindine-6-carboxylic acid

: 198279-45-7,224448-58-2
J 104132

Guidance literature:: With chromium(VI) oxide; periodic acid; In water; at -3 - 0 ℃;
DOI:10.1021/jo991292t

Reference yield:

: 258349-59-6
5-benzo[1,3]dioxol-5-yl-2-butyl-7-{2-[3-(tert-butyl-dimethyl-silanyloxy)-2-methyl-propyl]-4-methoxy-phenyl}-6,7-dihydro-5H-[1]pyrindine-6-carboxylic acid tert-butyl ester

: 198279-45-7,224448-58-2
J 104132

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / 20 - 25 °C

2: 10.9 g / H₅IO₆; CrO₃ / H₂O / -3 - 0 °C

With chromium(VI) oxide; hydrogenchloride; periodic acid; In water; 1: Hydrolysis / 2: Oxidation;
DOI:10.1021/jo991292t

Reference yield:

: (5R,6S,7R)-5-Benzo[1,3]dioxol-5-yl-2-butyl-7-[2-(2-carboxy-propyl)-4-methoxy-phenyl]-6,7-dihydro-5H-[1]pyrindine-6-carboxylic acid

: 224448-58-2
[5S-[5α,6β,7α(R*)]]-2-butyl-5-(1,3-benzodioxol-5-yl)-7-[(2-carboxypropyl)-4-methoxyphenyl]-6-dihydro-5H-cyclopenta[b]pyridine-6-carboxylic acid

Guidance literature:: With hydrogenchloride; mannitol; sodium citrate; at 40 ℃; pH=7.5; Further Variations:; pH-values; Temperatures; Equilibrium constant;
DOI:10.1248/cpb.49.1