η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride

Base Information

• Chemical Name: η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride
• CAS No.: 208035-95-4
• Molecular Formula: C₂₃H₂₂Cl₂SiZr
• Molecular Weight: 488.643

Synonyms:

Chemical Property of η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride

Chemical Property:

Purity/Quality:

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Technology Process of η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride

There total 1 articles about η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(1,3-cyclopentadienyl)-1-(3-benzyl)indenyldimethylsilane + zirconium(IV) chloride (10026-11-6) → η(5)-[1-(3-benzyl)indenylidene]-η(5)-(1-cyclopentadienylidene)dimethylsilane-zirconium dichloride (208035-95-4)

Guidance literature:

With n-BuLi; In diethyl ether; hexane; byproducts: LiCl; Ar-atmosphere; stirring ligand soln. (in Et2O) with 2 equiv. of BuLi (inhexane, room temp., 8 h), addn. of 1 equiv. ZrCl4, stirring overnight; evapn., extn. into CH2Cl2, filtration off of LiCl, crystn. (hexane/CH2Cl2, -25°C);

DOI:10.1016/S0022-328X(98)00371-4

upstream raw materials:

zirconium(IV) chloride

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