C₃₂H₄₃NO₅SSi

Base Information

Chemical Name:C₃₂H₄₃NO₅SSi
CAS No.:1366423-12-2
Molecular Formula:C₃₂H₄₃NO₅SSi
Molecular Weight:581.849
Hs Code.:

C<sub>32</sub>H<sub>43</sub>NO<sub>5</sub>SSi

Synonyms:

Suppliers and Price of C₃₂H₄₃NO₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₄₃NO₅SSi

Chemical Property:

Purity/Quality:

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Technology Process of C₃₂H₄₃NO₅SSi

There total 8 articles about C₃₂H₄₃NO₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1366422-70-9
N-((2R,3R,4S)-1,3-bis(benzyloxy)-5-(tert-butyldimethylsilyloxy)-4-hydroxypentan-2-yl)-4-methylbenzenesulfonamide

: 1366423-12-2
C₃₂H₄₃NO₅SSi

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo202054g

Reference yield:

: 1366423-08-6
C₁₅H₂₁N₃O₄

: 1366423-12-2
C₃₂H₄₃NO₅SSi

Guidance literature:: Multi-step reaction with 6 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3: triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

4: hydrogenchloride; water / methanol / 40 °C

5: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

6: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; dmap; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; water; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; mineral oil; 6: Mitsunobu reaction;
DOI:10.1021/jo202054g

Reference yield:

: 1366423-14-4
C₂₂H₂₉NO₄

: 1366423-12-2
C₃₂H₄₃NO₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

2: hydrogenchloride; water / methanol / 40 °C

3: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

4: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; dmap; di-isopropyl azodicarboxylate; water; triethylamine; triphenylphosphine; In methanol; dichloromethane; 4: Mitsunobu reaction;
DOI:10.1021/jo202054g