NiCl((C₆H₅)2PO)2C₁₀H₅

Base Information

• Chemical Name: NiCl((C₆H₅)2PO)2C₁₀H₅
• CAS No.: 1374033-98-3
• Molecular Formula: C₃₄H₂₅ClNiO₂P₂
• Molecular Weight: 621.662
• Mol file: 1374033-98-3.mol

Synonyms:

Chemical Property of NiCl((C₆H₅)2PO)2C₁₀H₅

Chemical Property:

Purity/Quality:

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Technology Process of NiCl((C₆H₅)2PO)2C₁₀H₅

There total 1 articles about NiCl((C₆H₅)2PO)2C₁₀H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

((C6H5)2PO)2C10H6 (1374033-97-2) + nickel dichloride (83864-14-6) → NiCl((C6H5)2PO)2C10H5 (1374033-98-3)

Guidance literature:

In toluene; toluene soln. of phosphinite added dropwise to suspn. of NiCl2 in toluene, refluxed overnight; filtered over silica gel, washed with Et2O, pumped off to dryness; residue extd. with CH2Cl2, solvent removed under vac.; recrystd. from CH2Cl2/hexane; elem. anal.;

DOI:10.1016/j.ica.2011.12.052

upstream raw materials:

((C₆H₅)2PO)2C₁₀H₆

nickel dichloride