C₅₄H₆₇NO₂Si₂

Base Information

Chemical Name:C₅₄H₆₇NO₂Si₂
CAS No.:1379684-11-3
Molecular Formula:C₅₄H₆₇NO₂Si₂
Molecular Weight:818.302
Hs Code.:

C<sub>54</sub>H<sub>67</sub>NO<sub>2</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₅₄H₆₇NO₂Si₂

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Technology Process of C₅₄H₆₇NO₂Si₂

There total 4 articles about C₅₄H₆₇NO₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80278-94-0
1,2,3,3a,4,8b-hexahydrocyclopent[b]indole

: 1379684-11-3
C₅₄H₆₇NO₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; johnphos; sodium t-butanolate / toluene / Reflux

2.1: N-Bromosuccinimide / acetone / 5 h / 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

With N-Bromosuccinimide; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; tert.-butyl lithium; palladium diacetate; caesium carbonate; johnphos; sodium t-butanolate; In tetrahydrofuran; acetone; toluene; pentane;
DOI:10.1039/c2jm30978e

Reference yield:

: 1250863-85-4
7-bromo-1,2,3,3a,4,8b-hexahydro-4-(4-methylphenyl)-cyclopent-[b]indole

: 1379684-11-3
C₅₄H₆₇NO₂Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

1.2: 25 °C / Inert atmosphere

2.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

With bis(tri-tert-butylphosphine)palladium⁽⁰⁾; tert.-butyl lithium; caesium carbonate; In tetrahydrofuran; pentane;
DOI:10.1039/c2jm30978e

Reference yield:

: 106-38-7
para-bromotoluene

: 1379684-11-3
C₅₄H₆₇NO₂Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; johnphos; sodium t-butanolate / toluene / Reflux

2.1: N-Bromosuccinimide / acetone / 5 h / 20 °C / Inert atmosphere

3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.75 h / -78 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

4.1: bis(tri-tert-butylphosphine)palladium⁽⁰⁾; caesium carbonate / tetrahydrofuran / Reflux; Inert atmosphere

With N-Bromosuccinimide; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; tert.-butyl lithium; palladium diacetate; caesium carbonate; johnphos; sodium t-butanolate; In tetrahydrofuran; acetone; toluene; pentane;
DOI:10.1039/c2jm30978e