N-(Benzyloxycarbonyl)-N-(benzyloxycarboxamido)glycine ethyl ester

Base Information

• Chemical Name: N-(Benzyloxycarbonyl)-N-(benzyloxycarboxamido)glycine ethyl ester
• CAS No.: 100260-20-6
• Molecular Formula: C₂₀H₂₂N₂O₆
• Molecular Weight: 386.404
• European Community (EC) Number: 663-108-2

Synonyms:N-(BENZYLOXYCARBONYL)-N-(BENZYLOXYCARBOXAMIDO)GLYCINE ETHYL ESTER;AKOS024434749

Chemical Property of N-(Benzyloxycarbonyl)-N-(benzyloxycarboxamido)glycine ethyl ester

Chemical Property:

• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 10
• Exact Mass: 386.14778643
• Heavy Atom Count: 28
• Complexity: 501

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCOC(=O)CN(C(=O)OCC1=CC=CC=C1)NC(=O)OCC2=CC=CC=C2

Technology Process of N-(Benzyloxycarbonyl)-N-(benzyloxycarboxamido)glycine ethyl ester

There total 3 articles about N-(Benzyloxycarbonyl)-N-(benzyloxycarboxamido)glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydrazinyl acetic acid ethyl ester hydrochloride (6945-92-2) + dibenzyl dicarbonate (31139-36-3) → benzyl 2-(2-ethoxy-2-ethoxyethyl)-1-hydrazinecarboxylate (4503-58-6) + Nα-Benzyloxycarbonyl-hydrazinoessigsaeure-ethylester (4467-44-1) + Nα,Nβ-Bis-benzyloxycarbonyl-hydrazino-essigsaeure-ethylester (100260-20-6)

Guidance literature:

With 4-methyl-morpholine; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/0040-4039(91)85080-O

Reference yield:

2-hydrazinyl acetic acid ethyl ester hydrochloride (6945-92-2) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl 2-(2-ethoxy-2-ethoxyethyl)-1-hydrazinecarboxylate (4503-58-6) + Nα-Benzyloxycarbonyl-hydrazinoessigsaeure-ethylester (4467-44-1) + Nα,Nβ-Bis-benzyloxycarbonyl-hydrazino-essigsaeure-ethylester (100260-20-6)

Guidance literature:

With 4-methyl-morpholine; dmap; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/0040-4039(91)85080-O

Reference yield:

2-hydrazinyl acetic acid ethyl ester hydrochloride (6945-92-2) + benzyl chloroformate (501-53-1,94274-21-2) → Nα,Nβ-Bis-benzyloxycarbonyl-hydrazino-essigsaeure-ethylester (100260-20-6)

Guidance literature:

With potassium hydrogencarbonate;

upstream raw materials:

2-hydrazinyl acetic acid ethyl ester hydrochloride

dibenzyl dicarbonate

benzyl chloroformate

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