(N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

Base Information

Chemical Name:(N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)
CAS No.:142233-32-7
Molecular Formula:C₂₅H₂₃Cl₂NP₂Pt
Molecular Weight:665.398
Hs Code.:

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Chemical Property of (N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

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Technology Process of (N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

There total 2 articles about (N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 2960-43-2
bis(diphenylphosphino)methylamine

: 142233-32-7
(N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

Guidance literature:: In dichloromethane; acetone; addn. of 1 equiv. of ligand (in Me2CO) to Pt-complex (in CH2Cl2, during10 min, pptn.), stirring (1 h); filtration, washing (cold Et2O);
DOI:10.1039/DT9950000521

Reference yield:

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 2960-43-2
bis(diphenylphosphino)methylamine

: 142233-32-7
(N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

Guidance literature:: In CH₂Cl₂; (Ar), suspn.of Pt complex in CH2Cl2 treated with equivmolar amounts of phosphane, stirred for 2 d at room temp.; filtered, washed (CHCl3), dried (vac.);
DOI:10.1002/ejic.200900824

Reference yield:

: 6708-12-9
4,4-bis(hydroxymethyl)-1,2-diselenolane

: 142233-32-7
(N,N-bis(diphenylphosphanyl)methylamine)dichloridoplatinum(II)

: 1235561-18-8
(N,N-bis(diphenylphosphanyl)methylamine)(2,2-bis(hydroxymethyl)-1,3-diselenolato)platinum(II)

Guidance literature:: With NaBH₄; HCl; K₂CO₃; In ethanol; (Ar), selenolane dissolved in C2H5OH treated with 3 equiv. of NaBH4 under stirring for 30 min, treated dropwise with 4 N HCl, stirred for 5 min,treated with excess K2CO3 and metal complex in acetone, stirred at room temp. overnight; evapd.(vac.), chromy.(silica gel);
DOI:10.1002/ejic.200900824