1-tert-butyl-1,2,3,4,5-pentaphenylstannole

Base Information

Chemical Name:1-tert-butyl-1,2,3,4,5-pentaphenylstannole
CAS No.:431063-51-3
Molecular Formula:C₃₈H₃₄Sn
Molecular Weight:609.398
Hs Code.:

Synonyms:

Suppliers and Price of 1-tert-butyl-1,2,3,4,5-pentaphenylstannole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-tert-butyl-1,2,3,4,5-pentaphenylstannole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-tert-butyl-1,2,3,4,5-pentaphenylstannole

There total 3 articles about 1-tert-butyl-1,2,3,4,5-pentaphenylstannole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 365449-70-3
1-bromo-4-(dibromophenylstannyl)-1,2,3,4-tetraphenyl-1,3-butadiene

: 431063-51-3
1-tert-butyl-1,2,3,4,5-pentaphenylstannole

: 431063-50-2
di(1,2,3,4,5-pentaphenyl-1-stanna-cyclopentadienyl)

Guidance literature:: With t-BuLi; In tetrahydrofuran; pentane; (Ar), t-BuLi in pentane added at -100°C to Sn complex in THF, warmed to room temp. over 4 h; evapd., chromy.(SiO2 - hexane/ethyl acetate 10:1), elem. anal.;
DOI:10.1002/ejic.200500274

Reference yield: 58.0%

: 365449-70-3
SnBr₂(C₆H₅)C(C₆H₅)C(C₆H₅)C(C₆H₅)CBr(C₆H₅)

: 594-19-4
tert.-butyl lithium

: 431063-51-3
1-tert-butyl-1,2,3,4,5-pentaphenylstannole

: 431063-50-2
di(1,2,3,4,5-pentaphenyl-1-stanna-cyclopentadienyl)

Guidance literature:: In tetrahydrofuran; Sn compound treated with 2 equiv. t-BuLi at -90°C; chromy.;
DOI:10.1039/b200238h

Reference yield:

: 431063-50-2
di(1,2,3,4,5-pentaphenyl-1-stanna-cyclopentadienyl)

: 594-19-4
tert.-butyl lithium

: 74-88-4
methyl iodide

: 431063-52-4
1-methyl-1,2,3,4,5-pentaphenylstannole

: 431063-51-3
1-tert-butyl-1,2,3,4,5-pentaphenylstannole

Guidance literature:: In not given; Sn compound treated with tert-BuLi at -80 °C; addn. of CH3I at room temp.; detected by H-NMR spectroscopy;
DOI:10.1039/b200238h