C₁₆H₁₉NO₇

Base Information

Chemical Name:C₁₆H₁₉NO₇
CAS No.:1613623-86-1
Molecular Formula:C₁₆H₁₉NO₇
Molecular Weight:337.329
Hs Code.:

C<sub>16</sub>H<sub>19</sub>NO<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₉NO₇

Chemical Property:

Purity/Quality:

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Technology Process of C₁₆H₁₉NO₇

There total 1 articles about C₁₆H₁₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Z)-5-(2,3-dimethoxy-3-oxoprop-1-en-1-yl)-2-hydroxybenzoic acid

: 56-12-2
4-amino-n-butyric acid

: 1613623-86-1
C₁₆H₁₉NO₇

Guidance literature:: (Z)-5-(2,3-dimethoxy-3-oxoprop-1-en-1-yl)-2-hydroxybenzoic acid; With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 25 ℃; for 12h;

4-amino-n-butyric acid; With triethylamine; In tetrahydrofuran; at 25 ℃; for 18h;
DOI:10.1002/anie.201400529

Reference yield:

: 1613623-86-1
C₁₆H₁₉NO₇

: (Z)-6-(carboxyformamido)-2-(3-(3-((3-carboxypropyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylamido)hexanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 14 h / 25 °C

2.1: sodium hydroxide / water; ethanol / 3 h / 25 °C

3.1: dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / tetrahydrofuran / 12 h / 25 °C

3.2: 18 h / 25 °C

4.1: acetic acid; hydrogen bromide / 0.1 h / 25 °C

5.1: potassium carbonate / water / 0.08 h / 25 °C

6.1: sodium hydroxide / 0.08 h / 25 °C

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen bromide; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1002/anie.201400529

Reference yield:

: 1613623-86-1
C₁₆H₁₉NO₇

: (Z)-2-(3-(3-((3-carboxypropyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylamido)-6-(2-ethoxy-2-oxoacetamido)hexanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 14 h / 25 °C

2.1: sodium hydroxide / water; ethanol / 3 h / 25 °C

3.1: dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / tetrahydrofuran / 12 h / 25 °C

3.2: 18 h / 25 °C

4.1: acetic acid; hydrogen bromide / 0.1 h / 25 °C

5.1: potassium carbonate / water / 0.08 h / 25 °C

With 1-hydroxy-pyrrolidine-2,5-dione; hydrogen bromide; potassium carbonate; acetic acid; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1002/anie.201400529