(6S)-6-methyloctanoic acid

Base Information

• Chemical Name: (6S)-6-methyloctanoic acid
• CAS No.: 97749-11-6
• Molecular Formula: C₉H₁₈O₂
• Molecular Weight: 158.241

Synonyms:

Chemical Property of (6S)-6-methyloctanoic acid

Chemical Property:

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Technology Process of (6S)-6-methyloctanoic acid

There total 21 articles about (6S)-6-methyloctanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(S)-(+)-6-methyl-1-octanol (110453-78-6) → (6S)-6-methyloctanoic acid (504-99-4,928-30-3,97749-11-6,150950-00-8)

Guidance literature:

With sodium chlorite; sodium dihydrogenphosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In water; acetonitrile; at 20 ℃; for 16h;

DOI:10.1021/jo202642a

Reference yield: 50.0%

leustroducsin B (145142-82-1) → (6S)-6-methyloctanoic acid (504-99-4,928-30-3,97749-11-6,150950-00-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1016/S0040-4020(02)00528-8

Reference yield:

(S)-6-methyloctanal (37179-47-8) → (6S)-6-methyloctanoic acid (504-99-4,928-30-3,97749-11-6,150950-00-8)

Guidance literature:

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 1h;

DOI:10.1039/c5ob00780a

upstream raw materials:

(S)-1-bromo-4-methylhexane

sodium diethylmalonate

(S)-(+)-6-methyl-1-octanol

(S)-4-methylhexanoic acid

Downstream raw materials:

(S)-6-Methyl-octanoic acid (1S,3R)-3-((1Z,3Z)-4-{(4R,6R)-6-[(E)-(R)-1-(2-allyloxycarbonylamino-ethyl)-3-((2S,3S)-3-ethyl-6-oxo-3,6-dihydro-2H-pyran-2-yl)-1-hydroxy-allyl]-2,2-dimethyl-[1,3]dioxan-4-yl}-buta-1,3-dienyl)-cyclohexyl ester

N-[(R)-4-benzyloxycarbonylamino-2-((S)-6-methyl-octanoylamino)-butyryl]-L_s-threonine

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