prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide

Base Information

• Chemical Name: prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide
• CAS No.: 78522-95-9
• Molecular Formula: C₁₂H₁₀F₄S
• Molecular Weight: 262.271
• Mol file: 78522-95-9.mol

Synonyms:

Chemical Property of prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide

There total 3 articles about prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

pentafluorophenyl-prop-2-enyl thioether (70168-12-6) → ethyl pentafluorophenyl sulphide (33288-21-0) + 5,6,7,8-tetrafluorothiochroman (78522-91-5) + 4,5,6,7-tetrafluoro-2,3-dihydro-2-methyl-1-benzothiophen (78522-90-4) + prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide (78522-95-9)

Guidance literature:

With N,N-diethylaniline; for 23h; Heating;

DOI:10.1039/P19810001659

Reference yield:

pentafluorophenylthiol (771-62-0) → prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide (78522-95-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / n-butyl-lithium / tetrahydrofuran; hexane / 0.33 h / -70 °C

2: 8 percent / NN-diethylaniline / 23 h / Heating

With n-butyllithium; N,N-diethylaniline; In tetrahydrofuran; hexane;

DOI:10.1039/P19810001659

Reference yield:

2,3,4,5-Tetrafluorobenzenethiol (3467-86-5) + allyl bromide (106-95-6) → prop-2-enyl 3,4,5,6-tetrafluoro-2-(prop-2-enyl)phenyl sulphide (78522-95-9)

Guidance literature:

With n-butyllithium; copper(l) chloride; In tetrahydrofuran; hexane; for 14.5h; Ambient temperature;

DOI:10.1039/P19810001659

upstream raw materials:

pentafluorophenyl-prop-2-enyl thioether

2,3,4,5-Tetrafluorobenzenethiol

allyl bromide

pentafluorophenylthiol