C₂₂H₂₂N₂O

Base Information

Chemical Name:C₂₂H₂₂N₂O
CAS No.:1613614-64-4
Molecular Formula:C₂₂H₂₂N₂O
Molecular Weight:330.429
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂N₂O

Chemical Property:

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Technology Process of C₂₂H₂₂N₂O

There total 6 articles about C₂₂H₂₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1613614-49-5
2-benzyl-2-ethyl-N-(quinolin-8-yl)butanamide

: 1613614-64-4
C₂₂H₂₂N₂O

Guidance literature:: With sodium benzoate; Duroquinone; copper(l) chloride; In o-xylene; at 160 ℃; Schlenk technique; Sealed tube;
DOI:10.1002/anie.201311263

Reference yield:

: 5343-57-7
2-ethyl-2-benzyl-butyric acid

: 1613614-64-4
C₂₂H₂₂N₂O

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 17 h / 0 - 20 °C

2: triethylamine / dichloromethane / 20 °C

3: copper(l) chloride; Duroquinone; sodium benzoate / o-xylene / 160 °C / Schlenk technique; Sealed tube

With sodium benzoate; oxalyl dichloride; Duroquinone; triethylamine; copper(l) chloride; In dichloromethane; o-xylene; N,N-dimethyl-formamide;
DOI:10.1002/anie.201311263

Reference yield:

: 816-11-5
2-ethyl-butyric acid methyl ester

: 1613614-64-4
C₂₂H₂₂N₂O

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: -78 - 20 °C

2.1: methanol; sodium hydroxide / 60 °C

3.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 17 h / 0 - 20 °C

4.1: triethylamine / dichloromethane / 20 °C

5.1: copper(l) chloride; Duroquinone; sodium benzoate / o-xylene / 160 °C / Schlenk technique; Sealed tube

With methanol; sodium benzoate; oxalyl dichloride; Duroquinone; triethylamine; copper(l) chloride; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; o-xylene; N,N-dimethyl-formamide;
DOI:10.1002/anie.201311263