4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

Base Information

Chemical Name:4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate
CAS No.:77143-95-4
Molecular Formula:C₁₄H₁₄N₂S*ClHO₄
Molecular Weight:342.803
Hs Code.:

Synonyms:

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Chemical Property of 4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

Chemical Property:

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Technology Process of 4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

There total 5 articles about 4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3337-86-8
quinazoline-4(3H)-thione

: 77143-95-4
4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 2percent aq. sodium hydroxide / ethanol / 3 h / Heating

2: methanol; diethyl ether

With sodium hydroxide; In methanol; diethyl ether; ethanol;

Reference yield:

: 77143-96-5
4-<(α-Hydroxycyclohexyl)thio>quinazoline

: 77143-95-4
4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: perchloric acid / methanol / 48 h / Ambient temperature; 1) conc. sulphuric acid (4 h) then HClO₄ in methanol, 2) PPA (4h, 150 deg C) then perchloric acid

2: 70 percent / 2percent aq. sodium hydroxide / ethanol / 3 h / Heating

3: methanol; diethyl ether

With sodium hydroxide; perchloric acid; In methanol; diethyl ether; ethanol;

Reference yield:

: 1521-51-3,113667-32-6
rac-3-bromocyclohexene

: 77143-95-4
4-<(α-Cyclohexenyl)thio>quinazoline-monoperchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 2percent aq. sodium hydroxide / ethanol / 3 h / Heating

2: methanol; diethyl ether

With sodium hydroxide; In methanol; diethyl ether; ethanol;