4-acetamidobenzyl methyl sulfide

Base Information

Chemical Name:4-acetamidobenzyl methyl sulfide
CAS No.:117760-01-7
Molecular Formula:C₁₀H₁₃NOS
Molecular Weight:195.285
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetamidobenzyl methyl sulfide

Chemical Property:

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Technology Process of 4-acetamidobenzyl methyl sulfide

There total 3 articles about 4-acetamidobenzyl methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 54293-04-8
4-aminobenzyl methyl sulfide

: 117760-01-7
4-acetamidobenzyl methyl sulfide

Guidance literature:: In acetic acid;
DOI:10.1016/0957-4166(95)00199-Y

Reference yield:

: 100-14-1
4-nitrobenzyl chloride

: 117760-01-7
4-acetamidobenzyl methyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 8.8 g / ethanol / 1 h / Heating

2: 1.4 g / conc. HCl, Sn / ethanol / 0.5 h / Heating

3: 100 percent / acetic acid

With hydrogenchloride; tin; In ethanol; acetic acid;
DOI:10.1016/0957-4166(95)00199-Y

Reference yield:

: 103-84-4
Acetanilid

: 33577-16-1
methyl methylsulfinylmethyl sulfide

: 65134-90-9
2'-<(Methylthio)methyl>acetanilide

: 117760-01-7
4-acetamidobenzyl methyl sulfide

Guidance literature:: aluminium trichloride; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) CH₂Cl₂, room temperature 2.) CH₂Cl₂, room temperature, 7 days;
DOI:10.1016/S0040-4039(00)82029-8