C₆₅H₉₇N₁₁O₈

Base Information

• Chemical Name: C₆₅H₉₇N₁₁O₈
• CAS No.: 1588517-35-4
• Molecular Formula: C₆₅H₉₇N₁₁O₈
• Molecular Weight: 1160.55
• Mol file: 1588517-35-4.mol

Synonyms:

Chemical Property of C₆₅H₉₇N₁₁O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₅H₉₇N₁₁O₈

There total 2 articles about C₆₅H₉₇N₁₁O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexanepropionic acid (701-97-3) + C27H32N2O6 (1588517-30-9) + (S)-N-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropyl)-N-((allyloxy)carbonyl)glycine (1588517-31-0) + C32H41N3O8 (1588517-32-1) + C37H39N3O8 (1588517-33-2) + propionic acid (802294-64-0,79-09-4) + isopentanoyl chloride (108-12-3) + phenylacetyl chloride (103-80-0) → C65H97N11O8 (1588517-35-4)

Guidance literature:

C₂₇H₃₂N₂O₆; With benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimethylamine borane; In dichloromethane; for 0.333333h;

cyclohexanepropionic acid; (S)-N-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropyl)-N-((allyloxy)carbonyl)glycine; C₃₂H₄₁N₃O₈; C₃₇H₃₉N₃O₈; propionic acid; isopentanoyl chloride; phenylacetyl chloride; Further stages;

DOI:10.1002/ejoc.201301841

Reference yield:

C70H104N11O10Pol → C65H97N11O8 (1588517-35-4)

Guidance literature:

With water; trifluoroacetic acid; for 2h; Rink amide resin

DOI:10.1002/ejoc.201301841

upstream raw materials:

cyclohexanepropionic acid

C₂₇H₃₂N₂O₆

(S)-N-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropyl)-N-((allyloxy)carbonyl)glycine

C₃₂H₄₁N₃O₈