C₃₉H₄₇N₇O₈

Base Information

• Chemical Name: C₃₉H₄₇N₇O₈
• CAS No.: 1584149-64-3
• Molecular Formula: C₃₉H₄₇N₇O₈
• Molecular Weight: 741.844
• Mol file: 1584149-64-3.mol

Synonyms:

Chemical Property of C₃₉H₄₇N₇O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₄₇N₇O₈

There total 3 articles about C₃₉H₄₇N₇O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C33H36N6O7 (1584149-62-1) → C39H47N7O8 (1584149-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / N,N-dimethyl-formamide / Inert atmosphere

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / Inert atmosphere

With piperidine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/anie.201309135

Reference yield:

N-(3-((2,4-dinitrophenyl)amino)propyl)-N-(3-aminopropyl)methyl amine (92585-03-0) → C39H47N7O8 (1584149-64-3)

Guidance literature:

Multi-step reaction with 3 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / acetonitrile / Inert atmosphere

2: piperidine / N,N-dimethyl-formamide / Inert atmosphere

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / Inert atmosphere

With piperidine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/anie.201309135

Reference yield:

Fmoc-Leu-OH (35661-60-0) + C18H26N6O5 (1584149-63-2) → C39H47N7O8 (1584149-64-3)

Guidance literature:

With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In acetonitrile; for 2h; Inert atmosphere;

DOI:10.1002/anie.201309135

upstream raw materials:

Fmoc-Leu-OH

C₁₈H₂₆N₆O₅

C₃₃H₃₆N₆O₇

N-(3-((2,4-dinitrophenyl)amino)propyl)-N-(3-aminopropyl)methyl amine

Downstream raw materials:

C₂₄H₃₇N₇O₆

C₃₀H₄₃N₇O₁₀