Technology Process of C15H18N2O3
There total 4 articles about C15H18N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid; nitric acid
2: hydrogenchloride; tin(ll) chloride / 50 °C
3: copper(II) sulfate; sodium hydroxide; zinc / water / Reflux
4: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C
5: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0 °C
With
hydrogenchloride; sulfuric acid; nitric acid; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; sodium hydroxide; zinc;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2011.11.078
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C
2: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0 °C
With
N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2011.11.078
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(II) sulfate; sodium hydroxide; zinc / water / Reflux
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 °C
3: N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0 °C
With
copper(II) sulfate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; zinc;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2011.11.078