[(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

Base Information

Chemical Name:[(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester
CAS No.:220573-04-6
Molecular Formula:C₂₄H₂₇NO₄
Molecular Weight:393.483
Hs Code.:

Synonyms:

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Chemical Property of [(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

Chemical Property:

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Technology Process of [(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

There total 12 articles about [(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 220573-04-6
[(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: NaH / dimethylformamide

2: TBAF / tetrahydrofuran

3: Hg(OAc)2 / Heating

4: diphenyl ether / Heating

5: NaClO₂, NaH₂PO₄, 2-methyl-2-butene / H₂O; 2-methyl-propan-2-ol

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; mercury(II) diacetate; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; diphenylether; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 220573-04-6
[(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) PPh₃, H₂O; 2.) NaH / 1.) THF; 2.) DMF

2: 80 percent / NaHCO₃ / diphenyl ether / Heating

3: NaH / dimethylformamide

4: TBAF / tetrahydrofuran

5: Hg(OAc)2 / Heating

6: diphenyl ether / Heating

7: NaClO₂, NaH₂PO₄, 2-methyl-2-butene / H₂O; 2-methyl-propan-2-ol

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; diphenylether; water; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 171824-23-0
(-)-(1S,4R,4aS,5R,8aR)-5-tert-Butyldimethylsilyloxy-1,4,4a,6,7,8a-hexahydro-endo-1,4-methanonaphthalen-8(5H)-one

: 220573-04-6
[(1R,6R)-6-(Benzyl-benzyloxycarbonyl-amino)-cyclohex-2-enyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 10 steps

1: 84 percent / NaBH₄ / methanol

2: 81 percent / diphenylphosphorylazide, DEAD, PPh₃ / tetrahydrofuran

3: 1.) PPh₃, H₂O; 2.) NaH / 1.) THF; 2.) DMF

4: 80 percent / NaHCO₃ / diphenyl ether / Heating

5: NaH / dimethylformamide

6: TBAF / tetrahydrofuran

7: Hg(OAc)2 / Heating

8: diphenyl ether / Heating

9: NaClO₂, NaH₂PO₄, 2-methyl-2-butene / H₂O; 2-methyl-propan-2-ol

With sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; diphenylether; water; N,N-dimethyl-formamide; tert-butyl alcohol;