6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin

Base Information

• Chemical Name: 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin
• CAS No.: 41159-39-1
• Molecular Formula: C₂₀H₈F₁₂N₂
• Molecular Weight: 504.278

Synonyms:

Chemical Property of 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin

Chemical Property:

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Technology Process of 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin

There total 2 articles about 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

2,2,2-Trimethoxy-5-phenyl-3,3-Bis(trifluormethyl)-2,3-dihydro-1,4,2λ5-oxazophosphol (33550-42-4) → 3,4-Dimethyl-2-phenyl-5,5-bis(trifluormethyl)-1-pyrrolin-4-carbonsaeure-ethylester + 3,4-Dimethyl-2-phenyl-5,5-bis(trifluormethyl)-1-pyrrolin-3-carbonsaeure-ethylester + syn/anti-3-Phenyl-4-<2,2,2-trifluor-1-trifluormethyl(ethylimino)>-1,1-bis(trifluormethyl)-1,4-dihydroisochinolin + 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin (41159-39-1)

Guidance literature:

With Ethyl tiglate; In toluene; for 18h; Further byproducts given; Heating;

Reference yield: 29.0%

ethyl (Z)-2-methyl-2-butenoate (16509-44-7,55514-48-2) + 2,2,2-Trimethoxy-5-phenyl-3,3-Bis(trifluormethyl)-2,3-dihydro-1,4,2λ5-oxazophosphol (33550-42-4) → 3,4-Dimethyl-2-phenyl-5,5-bis(trifluormethyl)-1-pyrrolin-4-carbonsaeure-ethylester + 3,4-Dimethyl-2-phenyl-5,5-bis(trifluormethyl)-1-pyrrolin-3-carbonsaeure-ethylester + syn/anti-3-Phenyl-4-<2,2,2-trifluor-1-trifluormethyl(ethylimino)>-1,1-bis(trifluormethyl)-1,4-dihydroisochinolin + 6,6,12,12-Tetrakis(trifluormethyl)-6,12-dihydrodibenzo<1,5>-naphthyridin (41159-39-1)

Guidance literature:

In toluene; for 18h; Further byproducts given; Heating;

upstream raw materials:

ethyl (Z)-2-methyl-2-butenoate

2,2,2-Trimethoxy-5-phenyl-3,3-Bis(trifluormethyl)-2,3-dihydro-1,4,2λ⁵-oxazophosphol

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