D-xylose diisobutyl dithioacetal

Base Information

Chemical Name:D-xylose diisobutyl dithioacetal
CAS No.:61329-59-7
Molecular Formula:C₁₃H₂₈O₄S₂
Molecular Weight:312.495
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-xylose diisobutyl dithioacetal

Chemical Property:

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Technology Process of D-xylose diisobutyl dithioacetal

There total 1 articles about D-xylose diisobutyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5328-37-0
L-arabinose

: 513-44-0
2-methylpropanethiol-1

: 4460-61-1,61329-59-7,66290-78-6,100895-97-4
L-Arabinose-diisobutyldithioacetal

Guidance literature:: With hydrogenchloride;
DOI:10.1246/bcsj.4.264

Reference yield:

: 61329-59-7
D-xylose diisobutyl dithioacetal

: 191792-34-4
Toluene-4-sulfonic acid (2S,3S,4R)-2-benzyloxymethyl-4-hydroxy-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / TsCl, pyridine / -15 °C / 1.) -15 deg C, 1.5 h, 2.) RT, 2 d

2: 82 percent / imidazole / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, 3 d

3: 80 percent / pyridine / 72 h / Ambient temperature

4: 85 percent / aq. HgCl₂, HgO / acetonitrile / 1 h / Ambient temperature

5: 95 percent / 10 M BH₃*Me₂S / diethyl ether / 2 h / Ambient temperature

6: 85 percent / NaH / tetrahydrofuran / 18 h / 50 °C

7: 94 percent / 48percent aq. HBr / acetonitrile / 2 h / Ambient temperature

With pyridine; 1H-imidazole; dimethylsulfide borane complex; hydrogen bromide; sodium hydride; p-toluenesulfonyl chloride; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0957-4166(97)00136-5

Reference yield:

: 61329-59-7
D-xylose diisobutyl dithioacetal

: 1,4;2,3-dianhydro-5-O-benzyl-L-ribitol

Guidance literature:: Multi-step reaction with 8 steps

1: 85 percent / TsCl, pyridine / -15 °C / 1.) -15 deg C, 1.5 h, 2.) RT, 2 d

2: 82 percent / imidazole / dimethylformamide / 1.) 0 deg C, 30 min, 2.) RT, 3 d

3: 80 percent / pyridine / 72 h / Ambient temperature

4: 85 percent / aq. HgCl₂, HgO / acetonitrile / 1 h / Ambient temperature

5: 95 percent / 10 M BH₃*Me₂S / diethyl ether / 2 h / Ambient temperature

6: 85 percent / NaH / tetrahydrofuran / 18 h / 50 °C

7: 94 percent / 48percent aq. HBr / acetonitrile / 2 h / Ambient temperature

8: 94 percent / t-BuOK / benzene / 2 h

With pyridine; 1H-imidazole; dimethylsulfide borane complex; potassium tert-butylate; hydrogen bromide; sodium hydride; p-toluenesulfonyl chloride; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/S0957-4166(97)00136-5