1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine

Base Information

Chemical Name:1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine
CAS No.:76292-70-1
Molecular Formula:C₂₈H₃₂N₄O₁₂
Molecular Weight:616.582
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine

Chemical Property:

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Technology Process of 1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine

There total 3 articles about 1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 6829-40-9
aminomalonic acid diethyl ester

: 555-16-8
4-nitrobenzaldehdye

: 76292-70-1,125660-53-9
1-di(ethoxycarbonyl)methyl-2,5-di(4'-nitrophenyl)-4,4-diethoxycarbonylimidazolidine

Guidance literature:: With sodium ethanolate; In ethanol; at 40 ℃; for 120h;
DOI:10.1016/S0040-4020(01)89100-6

Reference yield:

: 13433-00-6
diethyl aminomalonate hydrochloride

: 555-16-8
4-nitrobenzaldehdye

: 76292-70-1
1-(Bis-ethoxycarbonyl-methyl)-2,5-bis-(4-nitro-phenyl)-imidazolidine-4,4-dicarboxylic acid diethyl ester

Guidance literature:: With sodium ethanolate; In ethanol; at 40 ℃;
DOI:10.1016/S0040-4039(00)78997-0

Reference yield:

: 20538-21-0
α,α-diphenylindole-2-methanol

: 6829-40-9
aminomalonic acid diethyl ester

: 555-16-8
4-nitrobenzaldehdye

: 76292-77-8
C₁₄H₁₆N₂O₆

: 76292-70-1
1-(Bis-ethoxycarbonyl-methyl)-2,5-bis-(4-nitro-phenyl)-imidazolidine-4,4-dicarboxylic acid diethyl ester

Guidance literature:: aminomalonic acid diethyl ester; 4-nitrobenzaldehdye; With (R)-3,3'-di(anthracen-9-yl)-5,5',6,6',7,7',8,8'-octahydro-[1,1'-binaphthalene]-2,2'-diyl hydrogen phosphate; In m-xylene; at 25 ℃; for 1h; Molecular sieve;

α,α-diphenylindole-2-methanol; In m-xylene; at 80 ℃; for 15h; Molecular sieve;
DOI:10.1002/chem.201603049