(+/-)-N--valin-chlorid

Base Information

• Chemical Name: (+/-)-N--valin-chlorid
• CAS No.: 4910-30-9
• Molecular Formula: C₁₂H₁₄ClNO₂S
• Molecular Weight: 271.768
• Mol file: 4910-30-9.mol

Synonyms:

Chemical Property of (+/-)-N--valin-chlorid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-N--valin-chlorid

There total 6 articles about (+/-)-N--valin-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

valine ethyl ester (13893-45-3) → (+/-)-N--valin-chlorid (4910-30-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₂NH

2: aq. HCl

3: PCl₅

With hydrogenchloride; phosphorus pentachloride; diethylamine;

DOI:10.1002/hlca.19650480822

Reference yield:

phenyl chlorothioformate (13464-19-2) → (+/-)-N--valin-chlorid (4910-30-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₂NH

2: aq. HCl

3: PCl₅

With hydrogenchloride; phosphorus pentachloride; diethylamine;

DOI:10.1002/hlca.19650480822

Reference yield:

N-phenylsulfanylcarbonyl-DL-valine ethyl ester (4910-25-2) → (+/-)-N--valin-chlorid (4910-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl

2: PCl₅

With hydrogenchloride; phosphorus pentachloride;

DOI:10.1002/hlca.19650480822

upstream raw materials:

N-phenylsulfanylcarbonyl-L-valine

phenyl chlorothioformate

valine ethyl ester

N-phenylsulfanylcarbonyl-DL-valine ethyl ester

Downstream raw materials:

(+/-)-N--valin-diethylamid

N--DL-valin-