Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2

Base Information

Chemical Name:Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2
CAS No.:197768-87-9
Molecular Formula:C₃₉H₃₂Ni₂O₃P₄
Molecular Weight:789.956
Hs Code.:

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Chemical Property of Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2

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Technology Process of Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2

There total 1 articles about Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 28923-39-9
nickel(II) bromide dimethoxyethane

: 201230-82-2
carbon monoxide

: 152426-68-1
2-(diphenylphosphino)-3-methylphosphinine

: 197768-87-9
Ni2(μ-CO)(CO)2(μ-2-diphenylphosphino-3-methyl-phosphinine)2

Guidance literature:: With Zn; In tetrahydrofuran; byproducts: COD; CO-atmosphere; stirring equimolar amts. of Ni-complex and phosphine withexcess Zn (room temp., 1 h), bubbling N2 for 30 min; concn., extn. of COD into hexanes, dissoln. in C6H6, filtration (Celite), pptn. on concn., collection (filtration); elem. anal.;
DOI:10.1016/S0022-328X(97)00071-5