6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

Base Information

Chemical Name:6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide
CAS No.:161761-60-0
Molecular Formula:C₂₇H₄₀F₃N₃O₈S
Molecular Weight:623.691
Hs Code.:

6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

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Chemical Property of 6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

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Technology Process of 6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

There total 6 articles about 6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19879-84-6
tetraacetyl thioglucose

: 161761-60-0
6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / K₂CO₃ / acetone; H₂O / 1 h / Ambient temperature

2: 93 percent / aq. CaCl₂, Zn, 78percent aq. EtOH / 2 h / Heating

3: dicyclohexylcarbodiimide, pyridine / a) 4 deg C, 4 h, b) 20 deg C, 5 d

4: 72 percent / 67percent aq. EtOH, AV-17 ionexchange resin / 6 h / Ambient temperature

5: dicyclohexylcarbodiimide, pyridine / 120 h / 20 °C

With pyridine; ethanol; AV-17 ionexchange resin; potassium carbonate; dicyclohexyl-carbodiimide; calcium chloride; zinc; In water; acetone;

Reference yield:

: 407-91-0
6-(trifluoroacetamido)hexanoic acid

: 161761-59-7
1-deoxy-1--β-D-glucopyranose

: 161761-60-0
6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

Guidance literature:: With pyridine; dicyclohexyl-carbodiimide; at 20 ℃; for 120h;

Reference yield:

: 407-91-0
6-(trifluoroacetamido)hexanoic acid

: 161761-60-0
6-[6-(2,2,2-Trifluoro-acetylamino)-hexanoylamino]-hexanoic acid [4-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-ylsulfanylmethyl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide, pyridine / a) 4 deg C, 4 h, b) 20 deg C, 5 d

2: 72 percent / 67percent aq. EtOH, AV-17 ionexchange resin / 6 h / Ambient temperature

3: dicyclohexylcarbodiimide, pyridine / 120 h / 20 °C

With pyridine; ethanol; AV-17 ionexchange resin; dicyclohexyl-carbodiimide;