C₂₇H₄₂N₆*6C₇H₈O₃S

Base Information

Chemical Name:C₂₇H₄₂N₆*6C₇H₈O₃S
CAS No.:109774-85-8
Molecular Formula:6C₇H₈O₃S*C₂₇H₄₂N₆
Molecular Weight:1483.9
Hs Code.:

C<sub>27</sub>H<sub>42</sub>N<sub>6</sub>*6C<sub>7</sub>H<sub>8</sub>O<sub>3</sub>S

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Chemical Property of C₂₇H₄₂N₆*6C₇H₈O₃S

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Technology Process of C₂₇H₄₂N₆*6C₇H₈O₃S

There total 9 articles about C₂₇H₄₂N₆*6C₇H₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109774-72-3
C₅₄H₇₅N₃O₁₂S₃

: 109774-85-8
C₂₇H₄₂N₆*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / MeOH / pTsOH / 1 h / Ambient temperature

2: 98 percent / Et₃N / CH₂Cl₂ / 2 h / -78 - 25 °C

3: 65 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

4: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

5: ion exchange resin (basic form)

With methanol; ion exchange resin (basic form); hydrogen bromide; caesium carbonate; triethylamine; phenol; toluene-4-sulfonic acid; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 109774-85-8
C₂₇H₄₂N₆*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide

2: LiAlH₄

4: 65 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

5: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

6: ion exchange resin (basic form)

With lithium aluminium tetrahydride; sodium azide; ion exchange resin (basic form); hydrogen bromide; caesium carbonate; phenol; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6

Reference yield:

: 77372-56-6
1,3,5-tris(aminomethyl)benzene

: 109774-85-8
C₂₇H₄₂N₆*6C₇H₈O₃S

Guidance literature:: Multi-step reaction with 4 steps

2: 65 percent / Cs₂CO₃ / dimethylformamide / 7 h / 80 °C

3: 33percent HBr, phenol / acetic acid / 24 h / 40 °C

4: ion exchange resin (basic form)

With ion exchange resin (basic form); hydrogen bromide; caesium carbonate; phenol; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)85349-6