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Technology Process of NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3

NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3

Base Information
  • Chemical Name:NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3
  • CAS No.:81704-72-5
  • Molecular Formula:3C2F3O2*C15H37CoN7O3
  • Molecular Weight:761.545
  • Hs Code.:
NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5<sup>(3+)</sup>*3CF<sub>3</sub>COO<sup>(1-)</sup>=NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5(CF<sub>3</sub>COO)3

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Chemical Property of NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3
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Technology Process of NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3

There total 1 articles about NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Co(NH<sub>3</sub>)5(COOHCHNH<sub>2</sub>CH<sub>2</sub>CH(CH<sub>3</sub>)2)<sup>(3+)</sup>*3BF<sub>4</sub><sup>(1-)</sup>*2H<sub>2</sub>O=Co(NH<sub>3</sub>)5(COOHCHNH<sub>2</sub>CH<sub>2</sub>CH(CH<sub>3</sub>)2)(BF<sub>4</sub>)3*2H<sub>2</sub>O
81688-38-2

Co(NH3)5(COOHCHNH2CH2CH(CH3)2)(3+)*3BF4(1-)*2H2O=Co(NH3)5(COOHCHNH2CH2CH(CH3)2)(BF4)3*2H2O

L-Phe-Leu
3303-55-7

L-Phe-Leu

dicyclohexyl-carbodiimide
538-75-0

dicyclohexyl-carbodiimide

trifluoroacetic acid
76-05-1

trifluoroacetic acid

NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5<sup>(3+)</sup>*3CF<sub>3</sub>COO<sup>(1-)</sup>=NH<sub>3</sub>CHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>CONHCHCOOCH<sub>2</sub>CH(CH<sub>3</sub>)2Co(NH<sub>3</sub>)5(CF<sub>3</sub>COO)3
81704-72-5

NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(3+)*3CF3COO(1-)=NH3CHCH2C6H5CONHCHCOOCH2CH(CH3)2Co(NH3)5(CF3COO)3

Guidance literature:
With 4-methyl-morpholine; In dichloromethane; byproducts: dicyclohexylurea; Boc-L-Phe was dissolved in CH2Cl2, cooled to 0°C, DCC in CH2Cl2 at 0°C was added, stirred at 0°C for 2 h, filtered, filtrate was evapd. to dryness by rotary evaporator, solid was dissoled in DMF, solid Co-complex was added; mixt. was stirred, N-methylmorpholine was added, stirred at room temp. for 25 min, acidified by CF3COOH, evapd. to dryness, EtAc was added, organic layer was extd. with aq. HAc, sepd., purified by exchange column, concd., column was washed with H2O;
DOI:10.1021/ja00378a021
upstream raw materials:

Co(NH3)5(COOHCHNH2CH2CH(CH3)2)(3+)*3BF4(1-)*2H2O=Co(NH3)5(COOHCHNH2CH2CH(CH3)2)(BF4)3*2H2O

L-Phe-Leu

dicyclohexyl-carbodiimide

trifluoroacetic acid

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