2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone

Base Information

Chemical Name:2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone
CAS No.:87497-99-2
Molecular Formula:C₁₄H₉Cl₂N₃O₂
Molecular Weight:322.15
Hs Code.:
DSSTox Substance ID:DTXSID301233475

Synonyms:2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone;DTXSID301233475;87497-99-2

Suppliers and Price of 2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:321.0071819
Heavy Atom Count:21
Complexity:415

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)CN=[N+]=[N-])OC2=C(C=C(C=C2)Cl)Cl

Technology Process of 2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone

There total 1 articles about 2-Azido-1-[2-(2,4-dichlorophenoxy)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.8%

: 86309-03-7
2-bromo-1-<2-(2,4-dichlorophenoxy)phenyl>ethanone

: 87497-99-2
2-azido-1-<2-(2,4-dichlorophenoxy)phenyl>ethanone

Guidance literature:: DOI:10.1039/P19830001483

Reference yield: 43.5%

: 87497-99-2
2-azido-1-<2-(2,4-dichlorophenoxy)phenyl>ethanone

: 149-73-5
trimethyl orthoformate

: 87498-00-8
2-azido-1-<2-(2,4-dichlorophenoxy)phenyl>-1,1-dimethoxyethane

Guidance literature:: acid;
DOI:10.1039/P19830001483

Reference yield:

: 87497-99-2
2-azido-1-<2-(2,4-dichlorophenoxy)phenyl>ethanone

: [2-(2,4-Dichloro-phenoxy)-phenyl]-acetic acid 3-methyl-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 43.5 percent / acid

2: 56 percent / hydrogen / 10percent palladium-on-charcoal / methanol / 18 h / 760 Torr

3: 3-methylbutyl nitrite, HCl gas. / 18 h / Ambient temperature; great caution when passing HCl (at -5 deg C)

With hydrogenchloride; hydrogen; isopentyl nitrite; palladium on activated charcoal; In methanol;
DOI:10.1039/P19830001483