Technology Process of 1-deutero-6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranose
There total 3 articles about 1-deutero-6-O-acetyl-2,3,4-tri-O-benzyl-α-D-mannopyranose which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium borodeuteride;
In
methanol; water;
at 0 ℃;
for 0.05h;
DOI:10.1021/jo070229y
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 73 percent / hydrazinium acetate / dimethylformamide
2: 93 percent / N-methylmorpholine N-oxide; tetrapropylammonium perruthenate; molecular sieves 3 Angstroem / CH2Cl2 / 2 h / 20 °C
3: sodium borodeuteride / methanol; H2O / 0.05 h / 0 °C
With
tetrapropylammonium perruthennate; sodium borodeuteride; 3 A molecular sieve; hydrazinium monoacetate; 4-methylmorpholine N-oxide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo070229y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 93 percent / N-methylmorpholine N-oxide; tetrapropylammonium perruthenate; molecular sieves 3 Angstroem / CH2Cl2 / 2 h / 20 °C
2: sodium borodeuteride / methanol; H2O / 0.05 h / 0 °C
With
tetrapropylammonium perruthennate; sodium borodeuteride; 3 A molecular sieve; 4-methylmorpholine N-oxide;
In
methanol; dichloromethane; water;
DOI:10.1021/jo070229y
