1-<2-phenyl>-2-thiocyanatopyrrole

Base Information

Chemical Name:1-<2-phenyl>-2-thiocyanatopyrrole
CAS No.:117954-66-2
Molecular Formula:C₂₁H₂₀ClN₃O₂S₂
Molecular Weight:445.994
Hs Code.:

1-<2-<N-(3-chloropropyl)-p-toluenesulphonylamino>phenyl>-2-thiocyanatopyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<2-phenyl>-2-thiocyanatopyrrole

Chemical Property:

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Technology Process of 1-<2-phenyl>-2-thiocyanatopyrrole

There total 3 articles about 1-<2-phenyl>-2-thiocyanatopyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 15192-76-4
copper(II) thiocyanate

: 117954-65-1
1-<2-phenyl>pyrrole

: 117954-66-2
1-<2-phenyl>-2-thiocyanatopyrrole

Guidance literature:: In ethanol; at 7 ℃; for 14h;

Reference yield:

: 99472-78-3
N-(2-toluene-p-sulphonamidophenyl)pyrrole sodium salt

: 117954-66-2
1-<2-phenyl>-2-thiocyanatopyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / dimethylformamide / 12 h / 120 °C

2: 53 percent / triphenylphosphine, CCl₄ / CHCl₃ / 12 h / Heating

3: 61 percent / ethanol / 14 h / 7 °C

With tetrachloromethane; triphenylphosphine; In ethanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 117954-64-0
1-<2-phenyl>pyrrole

: 117954-66-2
1-<2-phenyl>-2-thiocyanatopyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / triphenylphosphine, CCl₄ / CHCl₃ / 12 h / Heating

2: 61 percent / ethanol / 14 h / 7 °C

With tetrachloromethane; triphenylphosphine; In ethanol; chloroform;