tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate

Base Information

• Chemical Name: tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate
• CAS No.: 130277-80-4
• Molecular Formula: C₂₇H₃₆N₄O₉
• Molecular Weight: 560.604

Synonyms:

Chemical Property of tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate

There total 3 articles about tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

tert-butyl 5-acetamido-4,8-di-O-acetyl-6-azido-7,9-O-benzylidene-2,3,5,6-tetradeoxy-2-methylidene-D-glycero-D-talo-nononate → tert-butyl (3aS,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate + tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate (130277-80-4,130324-70-8,130324-72-0,130324-73-1)

Guidance literature:

In benzene; for 3h; Heating; further azido acetates;

DOI:10.1002/hlca.19900730422

Reference yield: 19.0%

tert-butyl 5-acetamido-4,8-di-O-acetyl-6-azido-7,9-O-benzylidene-2,3,5,6-tetradeoxy-2-methylidene-D-glycero-D-galacto-nononate → tert-butyl (3aS,5S,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate (130277-80-4,130324-70-8,130324-72-0,130324-73-1) + tert-butyl (3aR,5S,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate (130277-80-4,130324-70-8,130324-72-0,130324-73-1)

Guidance literature:

In benzene; for 4h;

DOI:10.1002/hlca.19900730422

Reference yield: 19.0%

tert-butyl 5-acetamido-4,8-di-O-acetyl-6-azido-7,9-O-benzylidene-2,3,5,6-tetradeoxy-2-methylidene-D-glycero-D-galacto-nononate → tert-butyl (3aS,5S,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate (130277-80-4,130324-70-8,130324-72-0,130324-73-1) + tert-butyl (3aR,5S,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate (130277-80-4,130324-70-8,130324-72-0,130324-73-1)

Guidance literature:

In benzene; for 4h;

DOI:10.1002/hlca.19900730422

Downstream raw materials:

tert-butyl (3R,4S,5S,6aS)-4-acetamido-5-acetoxy-3-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-1,3,4,5,6,6a-hexahydroazirino<1,2-a>pyridine-6a-carboxylate

tert-butyl 5-acetamido-2-C-(acetoxymethyl)-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-D-erythro-L-manno-nononate

tert-butyl 5-acetamido-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-manno-nononate

tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

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